BielefeldGED:Equipment: Difference between revisions
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== | == Diffractometer == | ||
The reconstructed ''Balzers Eldigraph KD-G2'' (one of only two still existing ones worldwide) is presently in use in the laboratory. | The reconstructed ''Balzers Eldigraph KD-G2'' (one of only two still existing ones worldwide) is presently in use in the laboratory. | ||
The most recent papers <bib id="BergerZFN2009" /> and <bib id="ReuterZNB2016" /> contain lots of details about this improved gas electron diffractometer. | The most recent papers <bib id="BergerZFN2009" /> and <bib id="ReuterZNB2016" /> contain lots of details about this improved gas electron diffractometer. | ||
=== Current state === | |||
<gallery heights=200px widths=200px mode="traditional"> | <gallery heights=200px widths=200px mode="traditional"> | ||
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</gallery> | </gallery> | ||
=== History === | |||
<gallery heights=200px widths=200px mode="traditional"> | <gallery heights=200px widths=200px mode="traditional"> | ||
File:Bielefeld_GED_Instrument_Apr2006.jpg|GED instrument in April 2006 (Uni-Münster) | File:Bielefeld_GED_Instrument_Apr2006.jpg|GED instrument in April 2006 (Uni-Münster) | ||
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</gallery> | </gallery> | ||
=== | === Sector === | ||
==== Backing Pumps | A sin<sup>2</sup>-type sector (15 cm in diameter, common formula is A*sin<sup>2</sup>(r/B)) is used. | ||
{| class="wikitable" | |||
| [[File:Bielefeld_Sector_2006.jpg|200px]] | |||
| [[File:Bielefeld_Sector_2013_1.jpg|200px]] | |||
| [[File:Bielefeld_Sector_2013_3.jpg|200px]] | |||
|} | |||
== Pumps == | |||
=== Backing Pumps === | |||
Backing (fore-vacuum) pumps: ''Edwards x05 Scrollpump Oilfree'', ''Edwards E2M80'' oil pump and ''Edwards EH500'' booster pump. Our last oilfree pump worked 48822.8 hours. On the pictures is the new one. | Backing (fore-vacuum) pumps: ''Edwards x05 Scrollpump Oilfree'', ''Edwards E2M80'' oil pump and ''Edwards EH500'' booster pump. Our last oilfree pump worked 48822.8 hours. On the pictures is the new one. | ||
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=== Diffusion Pumps === | |||
New diffusion pump (''Edwards Diffstak 250/2000P''), installed in December, 2013: | New diffusion pump (''Edwards Diffstak 250/2000P''), installed in December, 2013: | ||
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| [[File:Bielefeld_ODiffusionP_2013_2.jpg|200px]] | | [[File:Bielefeld_ODiffusionP_2013_2.jpg|200px]] | ||
|} | |} | ||
=== Turbo Pumps === | |||
Turbo pump (''Edwards EXT70H'') attached to the electron gun: | Turbo pump (''Edwards EXT70H'') attached to the electron gun: | ||
{| class="wikitable" | {| class="wikitable" | ||
| [[File:Bielefeld_TurboP_2013_1.jpg|200px]] | | [[File:Bielefeld_TurboP_2013_1.jpg|200px]] | ||
|} | |} | ||
== Inlet Systems == | |||
=== Room-temperature Nozzle === | |||
{| style="border: 0px;" | {| style="border: 0px;" | ||
|- valign="bottom" | |- valign="bottom" | ||
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=== Medium-temperature Nozzle === | |||
This nozzle has been constructed for evaporation of compounds in a temperature range from 25 to 380 °C. However, it has also been successfully used for low temperatures below -15 °C. | This nozzle has been constructed for evaporation of compounds in a temperature range from 25 to 380 °C. However, it has also been successfully used for low temperatures below -15 °C. | ||
{| style="border: 0px;" | {| style="border: 0px;" | ||
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|} | |} | ||
== Cold Trap == | |||
Cold trap designed for using liquid nitrogen and installed from the opposite to the inlet system side. | Cold trap designed for using liquid nitrogen and installed from the opposite to the inlet system side. | ||
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|} | |} | ||
== In-line mass-spectrometer == | |||
A Hiden mass-spectrometer (PIC 1000 series, up to 2500 amu) with EPIC ion counting detector is attached to the electron diffraction unit. | A Hiden mass-spectrometer (PIC 1000 series, up to 2500 amu) with EPIC ion counting detector is attached to the electron diffraction unit. | ||
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|} | |} | ||
== Detection system == | |||
Imaging Plates (IP) are used for recording diffraction patterns. IPs are scanned with a Fuji BAS-1800II scanner and the signal is deleted using an eraser. | Imaging Plates (IP) are used for recording diffraction patterns. IPs are scanned with a Fuji BAS-1800II scanner and the signal is deleted using an eraser. | ||
Revision as of 12:53, 12 January 2016
This page contains description of equipment used by GED group in Bielefeld.
News
| Date | Record |
|---|---|
| 13 May 2015 | A valve for separation of the diffraction and mass-spectrometer chambers has been built. |
| 22 May 2014 | Hiden PIC 1000 series mass-spectrometer has been installed. |
| 28 Feb 2014 | A new booster pump (Edwards EH500) has been installed. |
| 20 Dec 2013 | A new diffusion pump (Edwards Diffstak 250/2000P) has been installed. |
Diffractometer
The reconstructed Balzers Eldigraph KD-G2 (one of only two still existing ones worldwide) is presently in use in the laboratory. The most recent papers <bib id="BergerZFN2009" /> and <bib id="ReuterZNB2016" /> contain lots of details about this improved gas electron diffractometer.
Current state
The Hiden MS has been setup as residual gas analyser and a touch-control-panel has been established
History
GED instrument in April 2006 (Uni-Münster)
The apparatus with new gun, power supply and recording system (image plates), Jun 2007
November 2007, the apparatus is already in Uni-Bielefeld
September 2009, more control devices
May 2011, heavily improved control panel
The instrument in 2012
December 2013, new pumps installed
May 2014, the Hiden MS was installed for first measurements
Sector
A sin2-type sector (15 cm in diameter, common formula is A*sin2(r/B)) is used.
|
|
|
Pumps
Backing Pumps
Backing (fore-vacuum) pumps: Edwards x05 Scrollpump Oilfree, Edwards E2M80 oil pump and Edwards EH500 booster pump. Our last oilfree pump worked 48822.8 hours. On the pictures is the new one.
Diffusion Pumps
New diffusion pump (Edwards Diffstak 250/2000P), installed in December, 2013:
|
|
|
Old diffusion pump:
|
|
Turbo Pumps
Turbo pump (Edwards EXT70H) attached to the electron gun:
|
Inlet Systems
Room-temperature Nozzle
Medium-temperature Nozzle
This nozzle has been constructed for evaporation of compounds in a temperature range from 25 to 380 °C. However, it has also been successfully used for low temperatures below -15 °C.
Cold Trap
Cold trap designed for using liquid nitrogen and installed from the opposite to the inlet system side.
|
In-line mass-spectrometer
A Hiden mass-spectrometer (PIC 1000 series, up to 2500 amu) with EPIC ion counting detector is attached to the electron diffraction unit.
Detection system
Imaging Plates (IP) are used for recording diffraction patterns. IPs are scanned with a Fuji BAS-1800II scanner and the signal is deleted using an eraser.
References
<biblist />